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Question
- (2 points) explain why a high rate of heating during melting point determination could result in a lower melting range than the actual. a high rate of heating during melting point determination could result
When heating at a high rate, heat may not distribute evenly within the sample. The thermometer might register a temperature increase before the entire sample has truly reached its melting - point equilibrium. This leads to an apparent lower melting range as the recorded melting onset and completion occur prematurely.
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A high rate of heating during melting point determination could result in a lower melting range than the actual because heat does not distribute evenly and the thermometer registers a temperature increase before the sample is in true melting - point equilibrium.